期刊
TETRAHEDRON
卷 67, 期 1, 页码 144-151出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2010.11.007
关键词
Salmochelin; Total synthesis; Aryl beta-C-glucoside
资金
- department of chemistry
- college of Natural Sciences at Shanghai University
- Shanghai Leading Academic Discipline Project [S30107]
Salmochelin S1, S2, MGE, DGE, and TGE were prepared through amide bond connection of an aryl C-glucosyl acyl chloride ((ArCOCl)-C-1) and serine ester amines, followed by hydrogenolysis of the per-benzylated precursors. Each synthesis employed a highly diastereoselective Ni-catalyzed Negishi approach to the aryl C-glycoside subunit. (C) 2010 Elsevier Ltd. All rights reserved.
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