期刊
TETRAHEDRON
卷 67, 期 34, 页码 6362-6368出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2011.05.124
关键词
2-Deoxyglycoside; Microwave; Glycosylation; endo-Glycal; Lewis acid
资金
- National Science Council of Taiwan [NSC97-2113-M-039-001, NSC97-2628-M-001-016-MY3]
- China Medical University, Taiwan [CMU98-NCTU-07]
alpha-2-Deoxyglycosides were synthesized in good to excellent yields by microwave-assisted reaction of endo-glycals with various O-nucleophiles in the presence of catalytic amount of AlCl3. These glycosyl additions occurred with high alpha-stereoselectivity and were complete in 5-35 min in 65-93% yield. (C) 2011 Elsevier Ltd. All rights reserved.
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