期刊
TETRAHEDRON
卷 67, 期 9, 页码 1709-1715出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2010.12.055
关键词
1,3-Thiazolidine-2-thiones; Primary amine; Carbon disulfide; Multicomponent reaction
An easy, efficient, and simple one-pot approach for the synthesis of 1,3-thiazolidine-2-thiones via multicomponent reaction is reported. The reaction of a primary amine with carbon disulfide in the presence of dibenzoylacetylene or bis(4-methyl-1-benzoyl)acetylene in a mixture of CH2Cl2 and H2O after 5 h, afforded the title compound as alkene diastereomers. (C) 2010 Elsevier Ltd. All rights reserved.
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