期刊
TETRAHEDRON
卷 67, 期 36, 页码 6939-6943出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2011.06.072
关键词
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资金
- Natural Science Foundation of China [20972047]
- Shanghai Municipal Education Commission
- Shanghai Education Development Foundation [09SG28]
- New Century Excellent Talents in University
- Ministry of Education, China [NCET-07-0283]
- '111' Project [B07023]
The stereoselective synthesis of C12 oxygenated marine scalaranic sesterterpene 16-deacetoxy-12-epi-scalarafuran acetate and its 14-epimer were described. A highly stereoselective intramolecular Diels Alder addition was designed as the key step to construct the ring D, and the absolute configurations of natural 16-deacetoxy-12-epi-scalarafuran acetate was supported by the X-ray diffraction analysis of single crystal of corresponding 16-deacetoxy-12-epi-scalarafuran. (C) 2011 Elsevier Ltd. All rights reserved.
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