期刊
TETRAHEDRON
卷 67, 期 31, 页码 5550-5555出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2011.05.123
关键词
Homocoupling; Palladium(II)-catalyzed; C-H bond activation; Thiazole; Oxazole
资金
- National Natural Science Foundation [20902111]
- Ministry of Education of China [NCET 2008]
- Fundamental Research Funds for the Central Universities [JKZ2009002, JKY2009013]
An efficient Pd(OAc)(2)-catalyzed homocoupling of thiazole-4-carboxylic or oxazole-4-carboxylic derivatives is described. It represents a facile and practical methodology to prepare bis-5,5'-thiazole (oxazole)-4,4'-dicarboxylic derivatives in good to excellent yields. This protocol tolerates a series of substitutions on the thiazole (oxazole) rings, including alkyl, carbonyl, and electron-withdrawing/donating group substituted phenyl groups. (C) 2011 Elsevier Ltd. All rights reserved.
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