4.4 Article

A short formal synthesis of three epimers of penmacric acid

期刊

TETRAHEDRON
卷 66, 期 32, 页码 6167-6173

出版社

PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2010.05.102

关键词

Penmacric acid; Epimers; Pyroglutamate; Lithium enolate; Titanium enolate

资金

  1. CSIR-UGC, New Delhi, India

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An extremely short formal synthesis of three epimers of penmacric acid is accomplished starting from pyroglutamate in one or two steps. Stereochemical outcome in the reaction of Li and Ti enolates of pyroglutamate with imines is found to be dependent on both chelation and steric factors. (C) 2010 Elsevier Ltd. All rights reserved.

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