期刊
TETRAHEDRON
卷 64, 期 51, 页码 11666-11672出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.tet.2008.10.017
关键词
Acid catalyst; Amberlite IR-120; Benzylation; Benzyl alcohol; Palladium coupling; 3,4-Disubstituted coumarin
资金
- CSIR, New Delhi
An efficient and operationally simple method for C3-alkylation of 4-hydroxycoumarins has been developed under acidic medium giving good yields of the products. In the present method, a reusable Amberlite (R) IR-120 (H(-) form) was used as an acid catalyst and secondary benzyl alcohols were used as alkylating agents. The obtained 3-alkylated-4-hydroxycoumarins offered an easy access for the synthesis of 3,4-dissubstituted coumarins by way of Pd-catalyzed coupling reactions. (C) 2008 Elsevier Ltd. All rights reserved.
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