期刊
SYNTHETIC COMMUNICATIONS
卷 39, 期 22, 页码 3982-3989出版社
TAYLOR & FRANCIS INC
DOI: 10.1080/00397910902883579
关键词
Aza-Michael reaction; HClO4; SiO2; hydroamination; microwave irradiation; reusable catalyst; solvent-free
资金
- Indian Institute of Chemical Technology-Aisin Cosmos Collaborative Research Project
Highly efficient solvent-free aza-Michael additions of a variety of amines to ,-unsaturated carbonyl compounds under microwave-irradiation conditions catalyzed by perchloric acid impregnated on silica gel (HClO4/SiO2) is reported. The reactions are completed within 2-7min in a microwave oven to produce the corresponding adducts in excellent yields, and the catalyst can be recovered and reused.
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