期刊
SYNTHESIS-STUTTGART
卷 50, 期 23, 页码 4611-4616出版社
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0037-1609554
关键词
phenylpropanoids; DDQ oxidation; 4-hydroxycinnamaldehydes; boropinal C; 7-methoxywutaifuranal
资金
- National Natural Science Foundation of China [21702002, 31640068]
- Anhui Provincial Natural Science Foundation [1808085QC79]
Phenylpropanoid natural products containing a cinnamaldehyde motif were easily synthesized from allylarenes mediated by 2,3-di-chloro-5,6-dicyano-1,4-benzoquinone (DDQ) oxidation. Representative examples described herein are five types of 4-hydroxycinnamaldehyde derivatives from monolignols biosynthesis, Boropinal C, and 7-methoxywutaifuranal from plant extracts. Especially, simple synthesis of 7methoxywutaifuranal was exploited through selective mono-oxidation and subsequent isomerization-ring-closing-metathesis strategy.
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