期刊
SYNTHESIS-STUTTGART
卷 44, 期 3, 页码 439-445出版社
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0031-1290066
关键词
expeditious synthesis; papilionaceous molecule; oligobenzofurans; ferric chloride; oxidative aromatic cyclization
资金
- National Basic Research Program of China (973 Program) [2010CB833200]
- National Natural Science Foundation of China [20972060, 21061160494]
- Specialized Research Fund for the Doctoral Program of Higher Education [20090211110007]
- 111 Project
An efficient synthetic route to construct particular papilionaceous molecules containing oligobenzofurans is described. The key steps involved composing the backbone of the molecules by the Sonogashira cross-coupling reaction, followed by closing the benzofuran ring under alkaline conditions, and further aromatic cyclization of a multi-benzofuranyl precursor using ferric chloride as the oxidative reagent. Basic optical studies (UV-Vis, fluorescence, and fluorescence quantum yield) have been carried out on the synthesized molecules.
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