3.9 Article

Synthesis and Characterization of Nanocrystalline In2O3 and Its Efficacy as a Catalyst for the One Pot Synthesis of Amidoalkyl Naphthols

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TAYLOR & FRANCIS INC
DOI: 10.1080/15533174.2012.740749

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amidoalkyl naphthol; indium oxide; multicomponent condensation; nanocatalyst

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In2O3 nanopaticles were synthesized by glycine-nitrate combustion method. The synthesized In2O3 is characterized by the powder X-ray diffraction and transmission electron microscopy. The average crystallite size, as determined by Scherrer's formula, was found to be about 48nm. A catalytic amount of In2O3 nanopaticles, were used for an efficient synthesis of amidoalkyl naphthols via multicomponent condensation of aryl aldehydes, -naphthol, and urea or acetamide. In2O3 nanopaticles were found to be highly active for the transformation with excellent yield and purity of the product in a short reaction time.

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