期刊
SYNLETT
卷 24, 期 16, 页码 2143-2147出版社
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0033-1339522
关键词
benzyne; magnesium; one-pot; tandem reaction; total synthesis
资金
- MEXT, Japan
- KAKENHI [21790006, 23790004]
- Cabinet Office, Government of Japan [LS008]
- Suntory Institute for Bioorganic Research
- Astellas Foundation for Research on Metabolic Disorders
- Banyu Life Science Foundation International
- Grants-in-Aid for Scientific Research [23790004, 21790006] Funding Source: KAKEN
A formal synthesis of a hepatitis C virus (HCV) inhibitor is described. The synthesis features a benzyne-mediated one-pot indoline formation-methylation sequence and an In(OTf)(3)-mediated mild oxa-Pictet-Spengler reaction for the synthesis of substituted electron-rich pyranoindole.
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