期刊
SYNLETT
卷 24, 期 10, 页码 1205-1210出版社
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0033-1338956
关键词
N-heterocyclic carbenes; catalysis; immobilization; amides; solid-phase synthesis
资金
- European Research Council [ERC] [306793 - CASAA]
- ETH Zurich
We have prepared an oligomeric histidine-bound N-heterocyclic carbene precursor by coupling a carboxylic acid functionalized 1,2,4-triazolium salt to a peptide using solid-phase peptide synthesis. We have demonstrated that the resulting multifunctional resin-bound catalyst cooperatively facilitates redox amidation reactions of aldehydes and amines, a reaction not catalyzed by N-heterocyclic carbenes alone.
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