期刊
SYNLETT
卷 -, 期 16, 页码 2315-2320出版社
GEORG THIEME VERLAG KG
DOI: 10.1055/s-0030-1261232
关键词
N-chlorosuccinimide; sulfonyl chlorides; sulfonamides; sulfonyl azides
资金
- Iran National Science Foundation (INSF)
- Payame Noor University (PNU)
A convenient synthesis of sulfonamides and sulfonyl azides from thiols is described. In situ preparation of sulfonyl chlorides from thiols is accomplished by oxidation with N-chlorosuccinimide (NCS), tetrabutylammonium chloride, and water. The sulfonyl chlorides are then further allowed to react with excess amine or sodium azide in the same reaction vessel.
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