期刊
SOLID STATE COMMUNICATIONS
卷 149, 期 45-46, 页码 2115-2119出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.ssc.2009.07.053
关键词
Nanostructures; Chemical synthesis; Scanning and transmission electron microscopy; Magnetic property
资金
- 973 Project of China [2005CB623601]
Fe3O4 hollow microsphere chains with lengths of 8-11 mu m have been solvothermally synthesized in the mixed solution of glycerol and water with 1 M NaOH. The hollow microspheres have diameters in the range 0.7-1 mu m, and the thickness of the shells is 150-300 nm. The shell of the hollow microspheres is constructed by octahedrons of 100-170 nm. However, when the concentration of NaOH is adjusted to 3 M, the octahedron chains with lengths of 30-50 mu m can be obtained. The magnetic saturation values of hollow microsphere chains and octahedron chains are 88.1 and 102.4 emu/g at room temperature, respectively. (C) 2009 Elsevier Ltd. All rights reserved.
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