期刊
SCIENCE AND TECHNOLOGY OF ADVANCED MATERIALS
卷 15, 期 5, 页码 -出版社
TAYLOR & FRANCIS LTD
DOI: 10.1088/1468-6996/15/5/055010
关键词
iron oxide; nanoparticles; synthesis; assembly; superlattice; mesocrystal
资金
- Swedish Research Council (VR)
- Knut and Alice Wallenberg (KAW) Foundation
- Nanomag FP-7 framework programme
Here we demonstrate how monodisperse iron oxide nanocubes and nanospheres with average sizes between 5 and 27 nm can be synthesized by thermal decomposition. The relative importance of the purity of the reactants, the ratio of oleic acid and sodium oleate, the maximum temperature, and the rate of temperature increase, on robust and reproducible size and shape-selective iron oxide nanoparticle synthesis are identified and discussed. The synthesis conditions that generate highly monodisperse iron oxide nanocubes suitable for producing large ordered arrays, or mesocrystals are described in detail.
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