期刊
RSC ADVANCES
卷 5, 期 24, 页码 18615-18621出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c4ra16268d
关键词
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资金
- Fujian Province Natural Science Foundation [2012D136]
- National Undergraduate Innovative Training Program [201410402002]
- Science and Technology Foundation of Fujian Provincial Bureau Quality and Technical Supervision [FJQI 2013108]
In this work, a novel sandwiched film of cadmium sulphide/reduced graphene oxide (CdS/r-GO) was synthesized via one step hydro-thermal reaction and electrodes modified with this composite were successfully used to simultaneously determine hydroquinone (HQ), catechol (CC) and resorcinol (RC). Additionally, some kinetic parameters, such as the charge transfer coefficient (alpha) and the electron transfer rate constant (k(s)) were calculated. Differential pulse voltammetry (DPV) was used for the simultaneous determination of HQ, CC and RC in their ternary mixture. The calibration curves of HQ, CC and RC were obtained in the ranges of 0.2 to 2300 mu M, 0.5 to 1350 mu M and 1.0 to 500 mu M, respectively. The detection limits for HQ, CC and RC were 0.054 mu M, 0.09 mu M and 0.23 mu M, respectively (S/N = 3). The modified electrode was then used to analyse tap water, well water and river water and the results show its significance for practical applications in the aquatic environment.
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