期刊
RUSSIAN JOURNAL OF INORGANIC CHEMISTRY
卷 57, 期 5, 页码 665-670出版社
MAIK NAUKA/INTERPERIODICA/SPRINGER
DOI: 10.1134/S0036023612050117
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资金
- Quaid-i-Azam University, Islamabad
New chloromono- and diorganotin(IV) complexes of 4-methyl-1-piperidine dithiocarboxylic acid have been synthesized in anhydrous chloroform. The complexes were characterized by microanalysis, IR, H-1 and C-13 NMR, mass spectrometry and XRD. The FTIR spectra clearly demonstrate that organotin(IV) moieties react with [S,S] atoms of the ligand. Compound (1) and (3) exhibits the 5-coordinated while the compound (2) exhibit 6-coordinated geometry in solid state. Compound (3) shows distorted trigonal bipyramidal geometry which is confirmed by X-ray single-crystal diffraction.
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