期刊
RUSSIAN JOURNAL OF INORGANIC CHEMISTRY
卷 56, 期 10, 页码 1532-1537出版社
MAIK NAUKA/INTERPERIODICA/SPRINGER
DOI: 10.1134/S003602361110024X
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资金
- Russian Foundation for Basic Research [09-03-0051, 09-03-12114]
- RF President Foundation [NSh-65264.2010.3]
Comparison of various laboratory procedures for the synthesis of palladium acetate demonstrated that the purest product containing no nitrite or nitrate impurities is formed in up to 90% yields upon the reaction of palladium nitrate with alkali metal acetates in aqueous acetic acid. Other laboratory syntheses are more labor-consuming and do not ensure high purity of the product. The synthesis by-products are described and possible reaction schemes are proposed.
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