期刊
RUSSIAN JOURNAL OF INORGANIC CHEMISTRY
卷 56, 期 11, 页码 1752-1756出版社
MAIK NAUKA/INTERPERIODICA/SPRINGER
DOI: 10.1134/S0036023611110027
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3-[(4-Chlorophenylamido)]propenoic acid has been synthesized by reaction of maleic anhydride and 4-chloroaniline in 1:1 molar ratio in glacial acetic acid and its metal complexes have been synthesized by the reaction of 3-[(4-chlorophenylamido)]propenoic acid with HgCl2 and [Zn(CH3COO)(2)] center dot 2H(2)O in 2: 1 molar ratio, respectively. All the synthesized compounds have been characterized by the elemental analysis, IR, UV/Vis and NMR (H-1, C-13) spectroscopy. Conductance for the reported compounds has been recorded in ethanol and suggests the non-electro lytic nature of complexes. IR data of metal complexes shows that the ligand is bound to the metal via both carboxylate oxygen atoms and complexes exhibits 4-coordinated geometry in solid state. NMR (H-1, C-13) study confirms the structure of the 3-[(4-chlorophenylamido)]propenoic acid and the reported complexes.
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