期刊
RUSSIAN JOURNAL OF INORGANIC CHEMISTRY
卷 53, 期 2, 页码 197-201出版社
MAIK NAUKA/INTERPERIODICA/SPRINGER
DOI: 10.1134/S0036023608020083
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General procedures for synthesis of anionic Cu(I) complexes with the closo-decaborate anion were worked out; they make it possible to prepare coordination compounds with a wide set of organic cations. The interaction of onium closo-decaborates with [Cu2B10H10] in acetonitrile acidified with anhydrous trifluoroacetic acid was found to be the most effective synthetic method that secures high yield and quality of the obtained products. The structure of {(C2H5)(3)NH[CuB10H10]} was determined by X-ray diffraction analysis.
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