期刊
MATERIALS
卷 8, 期 8, 页码 5336-5347出版社
MDPI
DOI: 10.3390/ma8085245
关键词
metal-organic frameworks; 1; 4-naphthalene dicarboxylate; nanoporous carbon; metal oxide nanoparticle; gas sorption
类别
资金
- Bureau of Energy of the Ministry of Economic Affairs, Taiwan
- Ministry of Science and Technology, Taiwan [MOST103-2632-M-033-001-MY3, MOST104-2113-M-033-006]
- Chung-Yuan Christian University
Three isostructural metal-organic frameworks, (MOFs), [Fe(OH)(1,4-NDC)] (1), [Al(OH)(1,4-NDC)] (2), and [In(OH)(1,4-NDC)] (3) have been synthesized hydrothermally by using 1,4-naphthalene dicarboxylate (1,4-NDC) as a linker. The MOFs were characterized using various techniques and further used as precursor materials for the synthesis of metal/metal oxide nanoparticles inserted in a carbon matrix through a simple thermal conversion method. The newly synthesized carbon materials were characterized by scanning electron microscopy, transmission electron microscopy, energy-dispersive X-ray spectroscopy analysis, powder X-ray diffraction and BET analysis. The results showed that the MOF-derived carbon composite materials maintained the morphology of the original MOF upon carbonization, and confirmed the insertion of metal/metal oxide particles in the carbon matrix.
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