期刊
RAPID COMMUNICATIONS IN MASS SPECTROMETRY
卷 24, 期 14, 页码 2109-2121出版社
WILEY
DOI: 10.1002/rcm.4621
关键词
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A simple procedure is described to identify acyl-glucuronides by coupled liquid chromatography/mass spectrometry after derivatization to a hydroxamic acid with hydroxylamine. The reaction specificity obviates the need for isolation of the acyl-glucuronide from an extract. Glucuronides derived from carbamic acids, and alkyl- and aromatic amines, are inert to the derivatization reaction conditions, making the hydroxamic acid derivative a fingerprint for acyl-glucuronides. Copyright (C) 2010 John Wiley & Sons, Ltd.
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