期刊
QUIMICA NOVA
卷 32, 期 6, 页码 1620-1634出版社
SOC BRASILEIRA QUIMICA
DOI: 10.1590/S0100-40422009000600046
关键词
QuEChERS method; food analysis; pesticides
QuEChERS - A MODERN SAMPLE PREPARATION METHOD FOR PESTICIDE MULTIRESIDUE DETERMINATION IN FOOD BY CHROMATOGRAPHIC METHODS COUPLED TO MASS SPECTROMETRY. This review attempts to provide an updated overview of the Quick, Easy, Cheap, Effective, Ruged and Safe (QuEChERS) multiresidue extraction method, that involves initial extraction in acetonitrile. an extraction/partition step after the addition of salt, and a cleanup step utilizing dispersive solid phase extraction. QuEChERS method is nowadays the most applied extraction method for the determination of pesticide residues in food samples. providing acceptable recoveries for acidic, neutral and basic pesticides. Several applications for various food matrices (fruits, vegetables, cereals and others) in combination with chromatographic mass spectrometry analysis were presented.
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