期刊
PROGRESS IN SOLID STATE CHEMISTRY
卷 42, 期 1-2, 页码 1-21出版社
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.progsolidstchem.2014.02.001
关键词
Scanning electron microscopy; Through-the-lens detection system; Nano-materials; Atmospheric SEM; Metal-organic frameworks; Mesoporous materials
资金
- JEOL (Japan)
- Grants-in-Aid for Scientific Research [25247053, 25287070] Funding Source: KAKEN
Research concerning nano-materials (metal-organic frameworks (MOFs), zeolites, mesoporous silicas, etc.) and the nano-scale, including potential barriers for the particulates to diffusion to/from is of increasing importance to the understanding of the catalytic utility. of porous materials when combined with any potential super structures (such as hierarchically porous materials). However, it is difficult to characterize the structure of for example MOFs via X-ray powder diffraction because of the serious overlapping of reflections caused by their large unit cells, and it is also difficult to directly observe the opening of surface pores using ordinary methods. Electron-microscopic methods including high-resolution scanning electron microscopy (HRSEM) have therefore become imperative for the above challenges. Here, we present the theory and practical application of recent advances such as through-the-lens detection systems, which permit a reduced landing energy and the selection of high-resolution, topographically specific emitted electrons, even from electrically insulating nano-materials. (c) 2014 Elsevier Ltd. All rights reserved.
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