4.7 Article

Biosynthesis of iron phosphate nanopowders

期刊

POWDER TECHNOLOGY
卷 194, 期 1-2, 页码 106-108

出版社

ELSEVIER SCIENCE BV
DOI: 10.1016/j.powtec.2009.03.034

关键词

Chemical synthesis; Biotemplate; Sintering; Nanostructured materials

资金

  1. Natural Science Foundation of China [B2052140, B5050470]
  2. Natural Science Foundation of Shandong, China [Y2008F39]

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Iron phosphate nanopowders; with flake morphologies have been synthesized by precipitation method with yeast cells as a biologic template, which provide the nucleation sites to regulate growth of FePO4 nanoparticles, XRD and TG-DSC show that pure and homogenous FePO4 crystal is synthesized at 543 degrees C. Transmission electron microscope (TEM) show that as-dried iron phosphate nanopowders contain a lot of organic matter and aggregate to yield clusters. The sample calcined at 600 degrees C shows flake shapes with length of 500-600 nm and width of 200-300 nm. Fourier transform infrared spectroscopy (FT-IR) is used to analyze the combination linkage of chemical bonds in organic-inorganic hybrid iron phosphate. Crown Copyright (C) 2009 Published by Elsevier B.V. All rights reserved.

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