A novel fluorescent monomer consisting of complementary amino and aldehyde functional groups was prepared via the Buchwald-Hartwig coupling protocol. The monomer self-condensed to yield a pi-conjugated regioregular polyazomethine that fluoresced in 48% in solution. The value measured by absolute methods is the highest reported fluorescence quantum yield for conjugated polyazomethines. The polymer was used a fluorimetric sensor for explosive analytes.
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