期刊
POLYMER BULLETIN
卷 71, 期 10, 页码 2523-2542出版社
SPRINGER
DOI: 10.1007/s00289-014-1205-3
关键词
Multi-walled carbon nanotube; D-Glucose; Transmission electron microscopy; Tensile properties; Thermal properties
资金
- Research Affairs Division of Isfahan University of Technology (IUT)
- National Elite Foundation (NEF)
- Center of Excellency in Sensors and Green Chemistry Research (IUT)
Functionalization of multi-walled carbon nanotubes (MWCNTs) by glucose was performed through esterification reaction. The reaction was carried out in water, in the presence of N,N'-carbonyldiimidazole as a catalyst. Glucose-functionalized MWCNTs (MWCNTs-Gl) were characterized by a set of methods including Fourier-transform infrared spectroscopy, X-ray diffraction, field emission scanning, and transmission electron microscopy. Thermogravimetric analysis (TGA) results also demonstrated the presence of organic portions of the functionalized MWCNTs. MWCNT-Gl/poly(amide-imide) (PAI) composite films with different MWCNTs-Gl content (5, 10, and 15 wt%) were prepared by ultrasonication-assisted solution blending method. Microscopic observations showed that the dispersion of the MWCNTs-Gl was improved by the organic groups on the MWCNT surface and functional groups on the PAI. TGA results showed that the hybrid films exhibited a good thermal stability. According to mechanical tensile tests, the tensile strength and the Young's modulus of the MWCNT-Gl/PAI composites were increased with increasing MWCNTs-Gl content.
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