期刊
PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS
卷 190, 期 7, 页码 1108-1114出版社
TAYLOR & FRANCIS LTD
DOI: 10.1080/10426507.2014.974091
关键词
Microwave irradiation; multicomponent reaction; beta-thiodiketone
资金
- National Basic Research Program of China under Grant 973 Program [2012CB214900]
An efficient synthesis of beta-thiodiketone derivatives using ammonium acetate as a catalyst, from mercaptans, aldehydes, and acetylacetone in an aqueous medium under the irradiation of microwave is described. Compared with the conventional refluxing conditions, the present method showed the advantages of simple work-up and shorter reaction times.
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