期刊
PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS
卷 184, 期 4, 页码 846-856出版社
TAYLOR & FRANCIS LTD
DOI: 10.1080/10426500802715551
关键词
CP cross-coupling reaction; phosphine-borane; vinylphosphine; vinyl tosylate
资金
- Ministere de la Recherche et des Nouvelles Technologies,
- CNRS (Centre National de la Recherche Scientifique)
- Region Basse-Normandie
- European Union (FEDER funding)
Vinylphosphine-borane complexes are efficiently synthesized by palladium-catalyzed CP cross-coupling of vinyl tosylates with diphenylphosphine-borane. Both activated and unactivated vinyl tosylates are successfully used. The vinylphosphine derivatives are purified by chromatography on silica gel.
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