期刊
ORGANOMETALLICS
卷 30, 期 19, 页码 5278-5283出版社
AMER CHEMICAL SOC
DOI: 10.1021/om2006613
关键词
-
资金
- Natural Science Foundation of China
- MOST of China [2011CB808601]
The first synthesis of trisubstituted guanidinium triflates has been achieved by a simple one-step procedure from readily available amines, carbodiimides, and Zn(OTf)(2). X-ray analysis revealed they adopt 1-D chain-like or novel 3-D hydrogen-bonded networks, which have not been reported previously in the solid structure of guanidinium salts. Isolation of a binuclear zinc complex and its subsequent carbodiimide insertion provide the insight into the mechanism for the formation of guanidinium triflates.
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