4.5 Article

Mechanistic Insight into the Reduction of Tertiary Phosphine Oxides by Ti(OiPr)4/TMDS

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ORGANOMETALLICS
卷 28, 期 22, 页码 6379-6382

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AMER CHEMICAL SOC
DOI: 10.1021/om900747b

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  1. Ph.D. grant
  2. Rhodia Operations

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The reduction mechanism of tertiary phosphine oxides by Ti(OiPr)(4)/hydrosiloxane was studied. Strong improvement was achieved using a drying agent. ESR spectra of the reaction mixture give evidence for a single electronic transfer (SET) mechanism.

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