期刊
ORGANIC PROCESS RESEARCH & DEVELOPMENT
卷 17, 期 12, 页码 1503-1509出版社
AMER CHEMICAL SOC
DOI: 10.1021/op400181g
关键词
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A scalable process for the preparation of high purity dimethyl 1,4-cubanedicarboxylate (3) is reported. The work described herein builds on previous synthetic work from this and other laboratories, to provide a reliable process that can be used to prepare multigram quantities of 3 in a partially telescoped, 8 step process, with minimal purification of intermediates.
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