期刊
ORGANIC PROCESS RESEARCH & DEVELOPMENT
卷 16, 期 5, 页码 1146-1149出版社
AMER CHEMICAL SOC
DOI: 10.1021/op200110a
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- Regione Veneto through FSE
- Fondazione Cariparo through MISCHA
Diazomethane is a valuable derivatizing agent but very difficult to handle for large-scale chemical transformations. We report here the base-induced decomposition of N-methyl-N-nitrosourea under continuous-flow conditions that enables the production up to 19 mol d(-1) of diazomethane, at a total flow rate of 53 mL min(-1).
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