期刊
ORGANIC PROCESS RESEARCH & DEVELOPMENT
卷 14, 期 1, 页码 205-214出版社
AMER CHEMICAL SOC
DOI: 10.1021/op900287j
关键词
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资金
- National Science Foundation [CHE-0847262]
- American Chemical Society Petroleum Research Fund [45433-AC1]
- University of Connecticut
- GlaxoSmithKline
- Division Of Chemistry [0847262] Funding Source: National Science Foundation
A new batch microwave reactor has been evaluated in the context of palladium-mediated transformations, condensation reactions, nucleophilic aromatic substitution reactions, and alkylations. Importantly, a linear scaling approach was taken, no changes being made to the protocol when moving from the small, developmental scale to larger scales. In some cases reactions were scaled over 18,000-fold when moving from small (0.1-1 nmol) to large (1-18 mol) runs.
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