期刊
ORGANIC PROCESS RESEARCH & DEVELOPMENT
卷 14, 期 6, 页码 1509-1513出版社
AMER CHEMICAL SOC
DOI: 10.1021/op100239n
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Phosgene is quantitatively formed from solid triphosgene in a solvent-free and safe process without fly reaction heat, catalyzed by planar N-heterocycles with deactivated imino functions. The rate of phosgene generation is adjustable to the rate of phosgene consumption in the subsequent phosgenation reaction by thermal control, catalyst concentration, and in some cases, specific properties of selected metal phthalocyanines. A thermal runaway reaction of this process is impossible.
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