期刊
ORGANIC LETTERS
卷 20, 期 16, 页码 5058-5061出版社
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.8b02221
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资金
- ANPCyT [PICT 2014-0445]
- CONICET [PIP 2012-0471, PUE IQUIR 2016]
- SECyT-UNR [BIO46]
Waltherione F was totally synthesized in seven steps and 31% overall yield from 2-nitro-3-methylanisole without the use of protecting groups. Key steps in the sequence were a Suzuki Miyaura coupling to attach the n-octyl chain and a microwave-promoted cyclization of an acetonyl anthranilate to give the heterocyclic core whose 3-OH was O-methylated.
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