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卷 16, 期 22, 页码 5854-5857出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol5027188
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资金
- York University
- Natural Sciences and Engineering Research Council (NSERC) of Canada
- Boehringer-Ingelheim Canada, Ltd.
The palladium-catalyzed cross-coupling reaction of cyclopropanol-derived ketone homoenolates with benzyl chlorides is reported. This reaction proceeds in high yields with electron-neutral and electron-rich benzyl chlorides; however, yields are low with electron-poor benzyl chlorides. In addition, a range of cyclopropanols can be coupled in good yields. The reaction can be conducted with a low catalyst loading (1% Pd) and on a gram scale without reduction in yield.
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