期刊
ORGANIC LETTERS
卷 16, 期 4, 页码 1060-1063出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol403591c
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资金
- Pfizer Worldwide Research and Development
- BP endowment
A sustainable flow chemistry process for the hydration of nitrites, whereby an aqueous solution of the nitrite is passed through a column containing commercially available amorphous manganese dioxide, has been developed. The product is obtained simply by concentration of the output stream without any other workup steps. The protocol described is rapid, robust, reliable, and scalable, and it has been applied to a broad range of substrates, showing a high level of chemical tolerance.
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