期刊
ORGANIC LETTERS
卷 16, 期 13, 页码 3508-3511出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol5014608
关键词
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资金
- Green Photonics Project in NAIST
- Program for Promoting the Enhancement of Research Universities in NAIST - Ministry of Education, Culture, Sports, Science and Technology, Japan
- [25288092]
- Grants-in-Aid for Scientific Research [25288092] Funding Source: KAKEN
The selective iodination of 2,7,12,17-tetrahexylporphycene 1 was successfully accomplished by using N-iodosuccinimide in the presence of activators to give 3-iodoporphycene 2 and 3,13-diiodoporphycene 3a. These iodinated porphycenes can be used as the substrates for palladium-catalyzed coupling to prepare porphycene-diketopyrrolopyrrole conjugates in two steps. The connection of the diketopyrrolopyrrole units to porphycenes broadened their absorption spectra and increased the intensity of the Q-bands due to the electronic interactions between the porphycene and diketopyrrolopyrrole moieties.
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