期刊
ORGANIC LETTERS
卷 16, 期 5, 页码 1398-1401出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol5001582
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资金
- Grants-in-Aid for Scientific Research [24106705, 25288016] Funding Source: KAKEN
3-Difluoromethylated 2,3-dihydrobenzoheteroles, 2,3-dihydrobenzofurans, 2,3-dihydrobenzothiophenes, and indolines were readily synthesized from ortho-heterosubstituted bromobenzenes, 2-bromophenols, 2-bromobenzenethiols, and 2-bromoanilines, respectively, in two steps: (1) gamma-selective allylic substitution of 3-bromo-3,3-difluoropropene with heteronucleophiles and (2) intramolecular radical cyclization of the resulting 3,3-difluoroallylic compounds.
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