4.8 Article

Highly Stereoselective Synthesis of Cyclopropylphosphonates Catalyzed by Chiral Ru(II)-Pheox Complex

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卷 16, 期 11, 页码 3012-3015

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AMER CHEMICAL SOC
DOI: 10.1021/ol501135p

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  1. Japan Society for the Promotion of Science [23550179]
  2. Grants-in-Aid for Scientific Research [23550179, 26288087] Funding Source: KAKEN

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Ru(II)-Pheox-catalyzed asymmetric cyclopropanation of diethyl diazomethylphosphonate with alkenes, including alpha,beta-unsaturated carbonyl compounds, afforded the corresponding optically active cyclopropylphosphonates in high yields and with excellent diastereoselectivity (up to 99:1) and enantioselectivity (up to 99% ee).

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