期刊
ORGANIC LETTERS
卷 16, 期 6, 页码 1634-1637出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol500260d
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资金
- NIH [GM058867]
- ACS Organic Division Fellowship
- predoctoral Ruth L. Kirschstein National Research Service Award
Difluorinated cyclooctynes are important reagents for labeling azido-biomolecules through copper-free click chemistry. Here, a safe, scalable synthesis of a difluorinated cyclooctyne is reported, which involves a key homologation/ring-expansion reaction. Sequential ring expansions were also employed to synthesize and study a novel difluorinated cyclononyne.
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