期刊
ORGANIC LETTERS
卷 16, 期 2, 页码 516-519出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol403398u
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资金
- NSF [CHE-0836757]
- Direct For Mathematical & Physical Scien [0836757] Funding Source: National Science Foundation
- Division Of Chemistry [0836757] Funding Source: National Science Foundation
A mild method for alpha-hydroxylation of N-acyl oxazolidinones by asymmetric radical addition of the 2,2,6,6-tetramethylpiperidine N-oxy (TEMPO) radical to titanium enolates was developed. The high diastereoselectivity and broad scope of the reaction show synthetic utility for the alpha-hydroxylation of substrates that are not tolerant to strongly basic conditions.
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