期刊
ORGANIC LETTERS
卷 15, 期 17, 页码 4520-4523出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol402034g
关键词
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资金
- MEXT [2105]
- Ube Foundation
- Grants-in-Aid for Scientific Research [21106001, 25410200, 25410115, 21106002] Funding Source: KAKEN
A new iterative one-pot sequential method for the solution-phase synthesis of oligosaccharides has been devised on the basis of the electrochemical oxidation of a propagating thioglycoside terminus to generate the corresponding triflate, followed by the reaction with a thioglycoside building block having a free hydroxyl group. A practical automated synthesizer was developed for the method and was effectively used for assembling up to six thioglycoside building blocks to synthesize partial structures of poly-beta-D-(1-6)-N-acetylglucosamine.
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