期刊
ORGANIC LETTERS
卷 15, 期 15, 页码 3950-3953出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol401727y
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资金
- Boehringer Ingelheim
- DuPont
- Eli Lilly
- Amgen
- AstraZeneca
- Roche
- Bristol-Myers Squibb
- Camille and Henry Dreyfus Foundation
- A. P. Sloan Foundation
- ACS GCI
- S. T. Li Foundation
- UCLA CSST Program
- Foote Family
- Pauley Family
- University of California, Los Angeles
- NSF [CHE-1048804]
- National Center for Research Resources [S10RR025631]
- Direct For Mathematical & Physical Scien
- Division Of Chemistry [1048804] Funding Source: National Science Foundation
The nickel-catalyzed Suzuki-Miyaura coupling of aryl halides and phenol-derived substrates with aryl boronic acids using green solvents, such as 2-Me-THF and tert-amyl alcohol, is reported. This methodology employs the commercially available and air-stable precatalyst, NiCl2(PCy3)(2), and gives biaryl products in synthetically useful to excellent yields. Using this protocol, bis(heterocyclic) frameworks can be assembled efficiently.
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