期刊
ORGANIC LETTERS
卷 16, 期 2, 页码 508-511出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol403393w
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-
资金
- National Natural Science Foundation of China [20872089, 21072129]
beta-Acylcoxy amides are prepared in moderate to high yields by palladium-catalyzed acyloxylation of primary sp(3) C-H bonds from simple amides without any special directing group. A catalytic system of Pd(OAc)(2)/CF3CO2H/K2S2O8 is available to various amides with N-substituted by linear alkanes, cyclic alkanes, and electron-deficient benzyl compounds in this reaction. Acyloxylated products could be transformed easily to the corresponding beta-hydroxy amides.
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