期刊
ORGANIC LETTERS
卷 15, 期 24, 页码 6132-6135出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol402982w
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资金
- University of South Carolina
- National Science Foundation CAREER Award [CHE-1055616]
- Division Of Chemistry
- Direct For Mathematical & Physical Scien [1055616] Funding Source: National Science Foundation
A silylation-based kinetic resolution has been developed for alpha-hydroxy lactones and lactams employing the chiral isothiourea catalyst (-)-benzotetramisole and triphenylsilyl chloride as the silyl source. The system is more selective for lactones than lactams, and selectivity factors up to 100 can be achieved utilizing commercially available reagents.
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