期刊
ORGANIC LETTERS
卷 14, 期 24, 页码 6278-6281出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol303041j
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资金
- EPSRC [EP/E055273/1]
- A*STAR
- German Academic Exchange Service (DAAD)
- EPSRC [EP/E055273/1] Funding Source: UKRI
- Engineering and Physical Sciences Research Council [EP/E055273/1] Funding Source: researchfish
The development of complementary palladium- and cobalt-catalyzed approaches to tricyclic arylsilanes suitable for elaboration into the CDE ring systems of rubriflordilactones A and B is reported. Microwave conditions are required to effect a cobalt-catalyzed triyne cyclotrimerization, which critically depends on the substitution pattern of the triyne termini. Mild conditions to elaborate these arylsilanes to the CDE cores of the natural products are described.
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