期刊
ORGANIC LETTERS
卷 14, 期 7, 页码 1684-1687出版社
AMER CHEMICAL SOC
DOI: 10.1021/ol3002267
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资金
- EPSRC
- EC [PIEF-GA-2009-254068]
- AstraZeneca
- Syngenta
- Engineering and Physical Sciences Research Council [EP/G007802/1] Funding Source: researchfish
- EPSRC [EP/G007802/1] Funding Source: UKRI
A synthetic strategy for the construction of the [7-5-5] all-carbon tricyclic core of numerous calyciphylline A-type Daphniphyllum alkaloids has been developed using a key intramolecular Pauson-Khand reaction. A subsequent base-mediated double-bond migration and a regio- and stereoselective radical late stage allylic oxygenation provide access to the substitution patterns of daphnilongeranin B and daphniyunnine D.
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